TA Instruments

AR1712-0001f

04/09/2012 17:13:39

Sample name	ASW 10 mm from base, 60 mm to top, disk 2 PMMA Br fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1712
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 17:13:39

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-21.82	7.415	-2.943	1.0000	22.4	790.3	5.3473	10000	0.1940	14.37	6.6842	668.42	3.384E-3	0.0	1.0	61.000	-66.947	5.932
1.153	12.23	0.09425	2.0000	22.4	796.9	13.1000	10000	0.1956	5.325	16.375	1637.5	3.383E-3	0.0	1.0	62.000	3.5373	9.787
1.719	19.32	0.08899	3.0000	22.4	791.1	27.1647	10000	0.1942	2.120	33.956	3395.6	3.383E-3	0.1	1.1	63.000	5.2743	15.45
2.341	22.99	0.1018	4.0000	22.4	787.0	40.6584	10000	0.1932	1.489	50.823	5082.3	3.383E-3	0.1	1.1	64.000	7.1814	18.39
3.789	30.81	0.1230	5.0000	22.4	794.4	67.6105	10000	0.1950	0.8371	84.513	8451.3	3.383E-3	0.1	1.1	65.000	11.626	24.64
5.719	39.45	0.1450	6.0000	22.4	803.5	106.5090	10000	0.1972	0.5163	133.14	13314	3.383E-3	0.1	1.1	66.000	17.545	31.56
6.424	42.51	0.1511	7.0000	22.4	796.9	126.1450	10000	0.1956	0.4410	157.68	15768	3.384E-3	0.1	1.1	67.000	19.708	34.01
8.301	49.11	0.1690	8.0000	22.4	777.1	165.3040	10000	0.1907	0.3222	206.63	20663	3.383E-3	0.1	1.1	68.000	25.468	39.29
10.95	57.52	0.1903	9.0000	22.4	793.6	223.0060	10000	0.1948	0.2399	278.76	27876	3.383E-3	0.2	1.2	69.000	33.580	46.02
12.53	62.87	0.1993	10.000	22.4	793.6	268.0110	10000	0.1948	0.2007	335.01	33501	3.384E-3	0.2	1.2	70.000	38.453	50.30
14.53	68.91	0.2109	11.000	22.4	797.7	319.3460	10000	0.1958	0.1680	399.18	39918	3.384E-3	0.2	1.2	71.000	44.584	55.13
16.52	74.43	0.2220	12.000	22.4	777.9	370.8130	10000	0.1909	0.1404	463.52	46352	3.384E-3	0.2	1.2	72.000	50.697	59.55
19.75	82.30	0.2399	13.016	22.4	772.9	453.5510	10000	0.1897	0.1141	566.94	56694	3.383E-3	0.2	1.2	73.016	60.588	65.84
22.17	88.10	0.2517	14.016	22.4	779.5	517.3880	10000	0.1913	0.1004	646.74	64674	3.383E-3	0.2	1.2	74.016	68.029	70.48
24.29	93.53	0.2597	15.016	22.4	767.1	581.0870	10000	0.1883	0.08770	726.36	72636	3.384E-3	0.3	1.3	75.016	74.525	74.82
28.03	101.4	0.2765	16.016	22.4	773.7	683.3550	10000	0.1899	0.07532	854.19	85419	3.384E-3	0.3	1.3	76.016	85.988	81.08
30.45	107.0	0.2845	17.016	22.4	762.2	759.6970	10000	0.1871	0.06655	949.62	94962	3.384E-3	0.3	1.3	77.016	93.425	85.62
33.47	112.4	0.2977	18.000	22.4	753.9	835.5810	10000	0.1850	0.05967	1044.5	1.0445E5	3.384E-3	0.3	1.3	78.000	102.67	89.92
36.23	117.5	0.3083	19.016	22.4	753.1	911.8390	10000	0.1848	0.05452	1139.8	1.1398E5	3.383E-3	0.3	1.3	79.016	111.15	94.02
39.77	125.8	0.3162	20.016	22.4	749.8	1045.2000	10000	0.1840	0.04738	1306.5	1.3065E5	3.384E-3	0.3	1.3	80.016	122.03	100.6
42.70	131.2	0.3256	21.000	22.4	748.9	1134.0699	10000	0.1838	0.04354	1417.6	1.4176E5	3.383E-3	0.4	1.4	81.000	131.00	104.9
45.14	136.3	0.3313	22.016	22.4	748.1	1223.4600	10000	0.1836	0.04028	1529.3	1.5293E5	3.383E-3	0.4	1.4	82.016	138.50	109.0
49.71	144.5	0.3441	23.016	22.4	738.2	1374.9900	10000	0.1812	0.03536	1718.7	1.7187E5	3.384E-3	0.4	1.4	83.016	152.52	115.6
52.51	149.8	0.3505	24.000	22.4	724.1	1476.9500	10000	0.1777	0.03226	1846.2	1.8462E5	3.384E-3	0.4	1.4	84.000	161.10	119.9
56.03	155.0	0.3616	25.000	22.4	727.5	1578.4000	10000	0.1785	0.03029	1973.0	1.9730E5	3.384E-3	0.4	1.4	85.000	171.90	124.0
60.13	162.8	0.3693	26.000	22.4	729.1	1742.3101	10000	0.1789	0.02750	2177.9	2.1779E5	3.384E-3	0.4	1.4	86.000	184.49	130.3
63.39	168.1	0.3770	27.000	22.4	725.0	1856.3199	10000	0.1779	0.02564	2320.4	2.3204E5	3.384E-3	0.5	1.5	87.000	194.49	134.5
66.96	175.8	0.3808	28.000	22.4	715.1	2028.5601	10000	0.1755	0.02313	2535.7	2.5357E5	3.384E-3	0.5	1.5	88.000	205.43	140.7
70.32	181.2	0.3881	29.016	22.4	716.7	2153.6799	10000	0.1759	0.02184	2692.1	2.6921E5	3.384E-3	0.5	1.5	89.016	215.74	144.9
74.91	186.5	0.4017	30.000	22.4	722.5	2280.2600	10000	0.1773	0.02077	2850.3	2.8503E5	3.384E-3	0.5	1.5	90.000	229.82	149.2
79.15	194.2	0.4076	31.016	22.4	721.7	2469.8401	10000	0.1771	0.01913	3087.3	3.0873E5	3.384E-3	0.5	1.5	91.016	242.83	155.4
82.59	199.3	0.4144	32.016	22.4	725.8	2602.6699	10000	0.1781	0.01827	3253.3	3.2533E5	3.384E-3	0.5	1.5	92.016	253.37	159.4
85.51	204.6	0.4179	33.000	22.4	702.7	2742.1299	10000	0.1725	0.01678	3427.7	3.4277E5	3.384E-3	0.6	1.6	93.000	262.33	163.7
90.86	212.4	0.4279	34.020	22.4	696.9	2950.2900	10000	0.1710	0.01545	3687.9	3.6879E5	3.383E-3	0.6	1.6	94.020	278.76	169.9
96.23	217.5	0.4425	35.008	22.4	700.2	3095.6299	10000	0.1718	0.01480	3869.5	3.8695E5	3.383E-3	0.6	1.6	95.008	295.24	174.0
100.2	222.8	0.4498	36.000	22.4	696.9	3248.2700	10000	0.1710	0.01404	4060.3	4.0603E5	3.383E-3	0.6	1.6	96.000	307.44	178.2
105.9	230.6	0.4592	37.016	22.4	683.6	3474.6699	10000	0.1678	0.01286	4343.3	4.3433E5	3.383E-3	0.6	1.6	97.016	324.80	184.4
108.8	235.6	0.4617	38.016	22.4	692.7	3626.3000	10000	0.1700	0.01248	4532.9	4.5329E5	3.384E-3	0.6	1.6	98.016	333.73	188.5
115.1	243.4	0.4728	39.000	22.4	669.6	3872.6299	10000	0.1643	0.01130	4840.8	4.8408E5	3.384E-3	0.7	1.7	99.000	353.07	194.7
119.8	248.6	0.4817	40.000	22.4	667.9	4037.8201	10000	0.1639	0.01081	5047.3	5.0473E5	3.383E-3	0.7	1.7	100.000	367.40	198.9
124.4	256.1	0.4858	41.016	22.4	653.9	4284.2900	10000	0.1605	9.966E-3	5355.4	5.3554E5	3.384E-3	0.7	1.7	101.016	381.76	204.9
126.7	261.3	0.4847	42.000	22.4	648.1	4459.8301	10000	0.1591	9.490E-3	5574.8	5.5748E5	3.383E-3	0.7	1.7	102.000	388.59	209.1
132.1	266.5	0.4955	43.000	22.4	644.8	4639.2700	10000	0.1583	9.078E-3	5799.1	5.7991E5	3.383E-3	0.7	1.7	103.000	405.17	213.2
139.2	274.1	0.5080	44.000	22.4	640.7	4901.5400	10000	0.1572	8.528E-3	6126.9	6.1269E5	3.384E-3	0.7	1.7	104.000	427.18	219.3
142.2	279.3	0.5090	45.016	22.4	636.5	5090.9399	10000	0.1562	8.160E-3	6363.7	6.3637E5	3.384E-3	0.8	1.8	105.016	436.16	223.4
149.0	287.1	0.5189	46.016	22.4	631.6	5374.9502	10000	0.1550	7.664E-3	6718.7	6.7187E5	3.384E-3	0.8	1.8	106.016	457.00	229.6
153.9	292.1	0.5267	47.016	22.4	615.0	5564.2500	10000	0.1510	7.208E-3	6955.3	6.9553E5	3.384E-3	0.8	1.8	107.016	472.02	233.7
157.8	297.2	0.5310	48.000	22.4	621.6	5760.8398	10000	0.1526	7.039E-3	7201.1	7.2011E5	3.384E-3	0.8	1.8	108.000	484.09	237.7
164.6	304.9	0.5397	49.000	22.4	620.8	6062.5000	10000	0.1524	6.676E-3	7578.1	7.5781E5	3.384E-3	0.8	1.8	109.000	504.93	244.0
169.4	310.0	0.5465	50.000	22.4	599.3	6264.3901	10000	0.1471	6.236E-3	7830.5	7.8305E5	3.384E-3	0.8	1.8	110.000	519.78	248.0
177.0	317.5	0.5575	51.000	22.4	602.6	6573.3901	10000	0.1479	5.976E-3	8216.7	8.2167E5	3.383E-3	0.9	1.9	111.000	543.13	254.0
180.5	322.7	0.5592	52.016	22.4	583.6	6787.8799	10000	0.1432	5.603E-3	8484.9	8.4849E5	3.383E-3	0.9	1.9	112.016	553.72	258.2
187.3	330.4	0.5669	53.000	22.4	575.3	7109.6001	10000	0.1412	5.272E-3	8887.0	8.8870E5	3.383E-3	0.9	1.9	113.000	574.57	264.3
192.6	335.4	0.5742	54.000	22.4	580.3	7330.2002	10000	0.1424	5.158E-3	9162.8	9.1628E5	3.384E-3	0.9	1.9	114.000	590.83	268.3
196.3	340.6	0.5765	55.000	22.4	550.5	7559.1001	10000	0.1351	4.746E-3	9448.9	9.4489E5	3.384E-3	0.9	1.9	115.000	602.37	272.5
203.8	348.2	0.5851	56.000	22.4	577.8	7899.6802	10000	0.1418	4.765E-3	9874.6	9.8746E5	3.383E-3	0.9	1.9	116.000	625.15	278.6
208.3	353.3	0.5898	57.016	22.4	541.5	8126.0200	10000	0.1329	4.339E-3	10158	1.0158E6	3.384E-3	1.0	2.0	117.016	639.20	282.6
217.1	361.0	0.6014	58.016	22.4	541.5	8486.0195	10000	0.1329	4.156E-3	10608	1.0608E6	3.384E-3	1.0	2.0	118.016	665.98	288.8
220.2	366.1	0.6015	59.016	22.4	543.9	8723.5703	10000	0.1335	4.059E-3	10904	1.0904E6	3.384E-3	1.0	2.0	119.016	675.50	292.8
228.8	373.6	0.6125	60.004	22.4	524.1	9082.7803	10000	0.1286	3.755E-3	11353	1.1353E6	3.384E-3	1.0	2.0	120.004	701.99	298.9

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

233.3	375.0	0.6220	1.0000	22.4	528.2	288.2280	10000	0.1296	3.756E-3	360.29	36029	3.384E-3	0.0	2.0	122.000	715.63	300.0
231.5	375.0	0.6174	2.0120	22.4	545.6	539.2670	10000	0.1339	3.880E-3	674.08	67408	3.384E-3	0.0	2.1	123.012	710.27	300.0
231.0	375.0	0.6160	3.0160	22.4	539.0	920.2480	10000	0.1323	3.833E-3	1150.3	1.1503E5	3.384E-3	0.1	2.1	124.016	708.75	300.0
231.9	375.0	0.6183	4.0120	22.4	517.5	1167.7400	10000	0.1270	3.680E-3	1459.7	1.4597E5	3.384E-3	0.1	2.1	125.012	711.32	300.0
232.9	375.0	0.6212	5.0120	22.4	502.6	1418.9700	10000	0.1234	3.574E-3	1773.7	1.7737E5	3.383E-3	0.1	2.1	126.012	714.63	300.0
236.6	375.0	0.6309	6.0120	22.4	510.0	1796.0601	10000	0.1252	3.627E-3	2245.1	2.2451E5	3.383E-3	0.1	2.1	127.012	725.83	300.0
233.7	375.0	0.6231	7.0160	22.4	520.8	2048.9600	10000	0.1278	3.703E-3	2561.2	2.5612E5	3.383E-3	0.1	2.1	128.016	716.89	300.0
229.9	375.0	0.6131	8.0120	22.4	496.0	2298.7600	10000	0.1217	3.527E-3	2873.5	2.8735E5	3.384E-3	0.1	2.2	129.012	705.40	300.0
231.5	375.0	0.6175	9.0120	22.4	539.0	2675.7400	10000	0.1323	3.833E-3	3344.7	3.3447E5	3.384E-3	0.2	2.2	130.012	710.37	300.0
231.9	375.0	0.6183	10.012	22.4	539.8	2926.8999	10000	0.1325	3.839E-3	3658.6	3.6586E5	3.383E-3	0.2	2.2	131.012	711.31	300.0
229.6	375.0	0.6122	11.012	22.4	498.5	3303.8899	10000	0.1223	3.545E-3	4129.9	4.1299E5	3.384E-3	0.2	2.2	132.012	704.31	300.0
229.6	375.0	0.6122	12.012	22.4	541.5	3557.1399	10000	0.1329	3.850E-3	4446.4	4.4464E5	3.384E-3	0.2	2.2	133.012	704.32	300.0
232.3	375.0	0.6195	13.012	22.4	515.8	3807.8401	10000	0.1266	3.668E-3	4759.8	4.7598E5	3.384E-3	0.2	2.2	134.012	712.77	300.0
230.1	375.0	0.6136	14.012	22.4	549.7	4190.5898	10000	0.1349	3.909E-3	5238.2	5.2382E5	3.384E-3	0.2	2.3	135.012	705.96	300.0
231.6	375.0	0.6176	15.012	22.4	534.8	4436.3101	10000	0.1313	3.803E-3	5545.4	5.5454E5	3.384E-3	0.3	2.3	136.012	710.56	300.0
231.5	375.0	0.6174	16.012	22.4	521.6	4811.9302	10000	0.1280	3.709E-3	6014.9	6.0149E5	3.383E-3	0.3	2.3	137.012	710.33	300.0
232.2	375.0	0.6193	17.012	22.4	529.9	5063.3198	10000	0.1301	3.768E-3	6329.2	6.3292E5	3.384E-3	0.3	2.3	138.012	712.48	300.0
229.5	375.0	0.6120	18.012	22.4	524.9	5314.7700	10000	0.1288	3.733E-3	6643.5	6.6435E5	3.384E-3	0.3	2.3	139.012	704.11	300.0
232.8	375.0	0.6208	19.012	22.4	526.6	5691.7002	10000	0.1292	3.745E-3	7114.6	7.1146E5	3.384E-3	0.3	2.3	140.012	714.17	300.0
233.3	375.0	0.6221	20.012	22.4	507.6	5944.0601	10000	0.1246	3.609E-3	7430.1	7.4301E5	3.384E-3	0.3	2.4	141.012	715.76	300.0
231.9	375.0	0.6183	21.012	22.4	518.3	6322.2300	10000	0.1272	3.686E-3	7902.8	7.9028E5	3.384E-3	0.4	2.4	142.012	711.31	300.0
229.6	375.0	0.6123	22.012	22.4	525.8	6573.7798	10000	0.1290	3.739E-3	8217.2	8.2172E5	3.384E-3	0.4	2.4	143.012	704.44	300.0
229.6	375.0	0.6124	23.012	22.4	507.6	6822.6201	10000	0.1246	3.609E-3	8528.3	8.5283E5	3.383E-3	0.4	2.4	144.012	704.52	300.0
229.9	375.0	0.6130	24.012	22.4	524.9	7199.8198	10000	0.1288	3.733E-3	8999.8	8.9998E5	3.383E-3	0.4	2.4	145.012	705.25	300.0
232.2	375.0	0.6192	25.012	22.4	534.0	7450.8398	10000	0.1311	3.798E-3	9313.6	9.3136E5	3.384E-3	0.4	2.4	146.012	712.42	300.0
228.9	375.0	0.6103	26.012	22.4	529.9	7702.3301	10000	0.1301	3.768E-3	9627.9	9.6279E5	3.383E-3	0.4	2.5	147.012	702.15	300.0
227.8	375.0	0.6075	27.012	22.4	546.4	8079.1299	10000	0.1341	3.886E-3	10099	1.0099E6	3.383E-3	0.5	2.5	148.012	698.97	300.0
231.8	375.0	0.6182	28.012	22.4	524.1	8330.7197	10000	0.1286	3.727E-3	10413	1.0413E6	3.383E-3	0.5	2.5	149.012	711.23	300.0
230.6	375.0	0.6149	29.012	22.4	514.2	8707.5195	10000	0.1262	3.656E-3	10884	1.0884E6	3.384E-3	0.5	2.5	150.012	707.39	300.0
229.3	375.0	0.6115	30.012	22.4	566.3	8958.7695	10000	0.1390	4.027E-3	11198	1.1198E6	3.384E-3	0.5	2.5	151.012	703.55	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

223.2	372.5	0.5994	1.0080	22.4	515.8	337.4440	10000	0.1266	3.718E-3	421.81	42181	3.384E-3	0.0	2.5	152.008	684.91	298.0
220.7	364.9	0.6048	2.0200	22.4	544.8	587.0010	10000	0.1337	4.091E-3	733.75	73375	3.384E-3	0.0	2.6	153.020	677.09	291.9
213.0	359.8	0.5919	3.0040	22.4	594.4	811.9710	10000	0.1459	4.591E-3	1015.0	1.0150E5	3.383E-3	0.1	2.6	154.004	653.41	287.8
205.6	352.1	0.5840	4.0240	22.4	539.8	1164.3500	10000	0.1325	4.354E-3	1455.4	1.4554E5	3.383E-3	0.1	2.6	155.024	630.84	281.7
199.5	347.1	0.5748	5.0160	22.4	573.7	1388.2900	10000	0.1408	4.761E-3	1735.4	1.7354E5	3.383E-3	0.1	2.6	156.016	612.18	277.7
196.0	339.5	0.5772	6.0200	22.4	541.5	1726.2000	10000	0.1329	4.697E-3	2157.8	2.1578E5	3.383E-3	0.1	2.6	157.020	601.27	271.6
188.0	334.3	0.5624	7.0200	22.4	558.8	1961.1801	10000	0.1372	4.999E-3	2451.5	2.4515E5	3.384E-3	0.1	2.6	158.020	576.92	267.5
182.4	326.8	0.5582	8.0200	22.4	614.2	2271.0300	10000	0.1507	5.751E-3	2838.8	2.8388E5	3.384E-3	0.1	2.7	159.020	559.66	261.4
176.0	321.7	0.5472	9.0040	22.4	601.0	2483.7400	10000	0.1475	5.806E-3	3104.7	3.1047E5	3.384E-3	0.2	2.7	160.004	540.08	257.4
173.7	316.6	0.5488	10.020	22.4	582.0	2696.5901	10000	0.1428	5.808E-3	3370.7	3.3707E5	3.384E-3	0.2	2.7	161.020	533.00	253.2
165.5	308.9	0.5357	11.028	22.4	599.3	3004.3999	10000	0.1471	6.281E-3	3755.5	3.7555E5	3.384E-3	0.2	2.7	162.028	507.66	247.1
160.2	303.8	0.5271	12.044	22.4	634.9	3203.7100	10000	0.1558	6.877E-3	4004.6	4.0046E5	3.383E-3	0.2	2.7	163.044	491.36	243.1
155.5	296.1	0.5251	13.016	22.4	615.0	3503.8401	10000	0.1510	7.015E-3	4379.8	4.3798E5	3.383E-3	0.2	2.7	164.016	476.98	236.9
149.8	290.9	0.5150	14.020	22.4	618.3	3697.9199	10000	0.1518	7.307E-3	4622.4	4.6224E5	3.383E-3	0.2	2.8	165.020	459.66	232.7
142.9	283.3	0.5045	15.024	22.4	641.5	3981.6899	10000	0.1574	7.991E-3	4977.1	4.9771E5	3.383E-3	0.3	2.8	166.024	438.48	226.7
139.1	278.1	0.5002	16.020	22.4	641.5	4167.2300	10000	0.1574	8.292E-3	5209.0	5.2090E5	3.384E-3	0.3	2.8	167.020	426.83	222.5
135.3	273.0	0.4957	17.056	22.4	618.3	4349.1201	10000	0.1518	8.299E-3	5436.4	5.4364E5	3.384E-3	0.3	2.8	168.056	415.14	218.4
129.3	265.4	0.4873	18.024	22.4	620.8	4611.2798	10000	0.1524	8.813E-3	5764.1	5.7641E5	3.384E-3	0.3	2.8	169.024	396.78	212.3
124.8	260.3	0.4794	19.020	22.4	642.3	4786.4302	10000	0.1576	9.483E-3	5983.0	5.9830E5	3.383E-3	0.3	2.8	170.020	382.82	208.2
119.7	252.4	0.4742	20.004	22.4	629.9	5043.8398	10000	0.1546	9.886E-3	6304.8	6.3048E5	3.384E-3	0.3	2.9	171.004	367.19	201.9
113.7	247.4	0.4594	21.020	22.4	662.1	5205.3599	10000	0.1625	0.01082	6506.7	6.5067E5	3.384E-3	0.4	2.9	172.020	348.73	197.9
111.6	242.3	0.4607	22.004	22.4	682.0	5367.8599	10000	0.1674	0.01162	6709.8	6.7098E5	3.384E-3	0.4	2.9	173.004	342.38	193.8
105.8	234.5	0.4514	23.024	22.4	672.9	5605.3599	10000	0.1652	0.01224	7006.7	7.0067E5	3.384E-3	0.4	2.9	174.024	324.70	187.6
101.7	229.4	0.4431	24.020	22.4	670.4	5755.3701	10000	0.1645	0.01273	7194.2	7.1942E5	3.384E-3	0.4	2.9	175.020	311.88	183.6
95.83	221.7	0.4322	25.024	22.4	674.5	5980.3398	10000	0.1656	0.01372	7475.4	7.4754E5	3.384E-3	0.4	2.9	176.024	294.01	177.4
92.19	216.4	0.4259	26.020	22.4	686.9	6130.2100	10000	0.1686	0.01466	7662.8	7.6628E5	3.384E-3	0.4	3.0	177.020	282.84	173.2
88.53	211.3	0.4189	27.020	22.4	687.8	6268.3501	10000	0.1688	0.01540	7835.4	7.8354E5	3.384E-3	0.5	3.0	178.020	271.59	169.1
82.84	203.7	0.4067	28.020	22.4	695.2	6474.6001	10000	0.1706	0.01676	8093.3	8.0933E5	3.384E-3	0.5	3.0	179.020	254.14	162.9
78.73	198.4	0.3968	29.016	22.4	710.9	6611.2100	10000	0.1745	0.01806	8264.0	8.2640E5	3.384E-3	0.5	3.0	180.016	241.54	158.7
75.04	193.1	0.3887	30.004	22.4	715.1	6805.8901	10000	0.1755	0.01918	8507.4	8.5074E5	3.383E-3	0.5	3.0	181.004	230.23	154.5
69.50	185.4	0.3748	31.020	22.4	728.3	6929.6602	10000	0.1787	0.02118	8662.1	8.6621E5	3.383E-3	0.5	3.0	182.020	213.22	148.3
67.05	180.1	0.3722	32.020	22.4	711.7	7054.3999	10000	0.1747	0.02193	8818.0	8.8180E5	3.383E-3	0.5	3.1	183.020	205.71	144.1
63.24	172.3	0.3670	33.020	22.4	718.4	7229.1499	10000	0.1763	0.02419	9036.4	9.0364E5	3.383E-3	0.6	3.1	184.020	194.02	137.9
60.03	167.2	0.3590	34.004	22.4	738.2	7342.3799	10000	0.1812	0.02640	9178.0	9.1780E5	3.383E-3	0.6	3.1	185.004	184.16	133.8
56.55	161.9	0.3492	35.020	22.4	724.1	7453.6699	10000	0.1777	0.02761	9317.1	9.3171E5	3.384E-3	0.6	3.1	186.020	173.49	129.6
52.20	153.8	0.3393	36.020	22.4	744.8	7615.7700	10000	0.1828	0.03147	9519.7	9.5197E5	3.384E-3	0.6	3.1	187.020	160.13	123.1
49.18	148.7	0.3306	37.024	22.4	738.2	7715.5601	10000	0.1812	0.03337	9644.5	9.6445E5	3.384E-3	0.6	3.1	188.024	150.87	119.0
46.39	143.5	0.3234	38.004	22.4	737.4	7815.2598	10000	0.1810	0.03583	9769.1	9.7691E5	3.384E-3	0.6	3.2	189.004	142.33	114.8
41.75	135.3	0.3085	39.020	22.4	736.5	7958.4102	10000	0.1808	0.04021	9948.0	9.9480E5	3.384E-3	0.7	3.2	190.020	128.09	108.3
39.36	130.3	0.3021	40.020	22.4	755.6	8045.5601	10000	0.1854	0.04453	10057	1.0057E6	3.384E-3	0.7	3.2	191.020	120.74	104.2
36.96	125.0	0.2957	41.028	22.4	754.7	8132.6499	10000	0.1852	0.04832	10166	1.0166E6	3.383E-3	0.7	3.2	192.028	113.40	99.98
33.23	116.8	0.2845	42.020	22.4	761.3	8257.1201	10000	0.1869	0.05579	10321	1.0321E6	3.384E-3	0.7	3.2	193.020	101.96	93.46
31.26	111.8	0.2797	43.024	22.4	751.4	8331.6201	10000	0.1844	0.06016	10415	1.0415E6	3.384E-3	0.7	3.2	194.024	95.912	89.41
28.63	106.5	0.2689	44.020	22.4	772.9	8406.2305	10000	0.1897	0.06817	10508	1.0508E6	3.384E-3	0.7	3.3	195.020	87.830	85.19
24.40	98.04	0.2489	45.024	22.4	770.4	8520.4697	10000	0.1891	0.08016	10651	1.0651E6	3.384E-3	0.8	3.3	196.024	74.860	78.43
22.11	92.75	0.2384	46.004	22.4	776.2	8579.9004	10000	0.1905	0.09023	10725	1.0725E6	3.384E-3	0.8	3.3	197.004	67.848	74.20
20.40	87.42	0.2333	47.020	22.4	791.9	8642.4297	10000	0.1944	0.1036	10803	1.0803E6	3.384E-3	0.8	3.3	198.020	62.579	69.94
18.46	81.76	0.2258	48.004	22.4	781.2	8703.7002	10000	0.1917	0.1169	10880	1.0880E6	3.383E-3	0.8	3.3	199.004	56.640	65.41
14.92	73.45	0.2031	49.008	22.4	780.4	8783.9600	10000	0.1915	0.1447	10980	1.0980E6	3.383E-3	0.8	3.3	200.008	45.773	58.76
13.38	68.04	0.1967	50.020	22.4	784.5	8833.2900	10000	0.1925	0.1694	11042	1.1042E6	3.383E-3	0.8	3.4	201.020	41.057	54.43
11.33	62.19	0.1821	51.020	22.4	777.9	8882.4600	10000	0.1909	0.2011	11103	1.1103E6	3.383E-3	0.9	3.4	202.020	34.752	49.75
9.776	56.18	0.1740	52.004	22.4	788.6	8925.4004	10000	0.1936	0.2498	11157	1.1157E6	3.383E-3	0.9	3.4	203.004	29.991	44.95
8.162	50.86	0.1605	53.024	22.4	788.6	8962.1797	10000	0.1936	0.3049	11203	1.1203E6	3.383E-3	0.9	3.4	204.024	25.040	40.68
6.579	44.93	0.1464	54.020	22.4	794.4	8998.7100	10000	0.1950	0.3934	11248	1.1248E6	3.383E-3	0.9	3.4	205.020	20.185	35.95
5.091	38.17	0.1334	55.020	22.4	790.3	9034.8496	10000	0.1940	0.5424	11294	1.1294E6	3.384E-3	0.9	3.4	206.020	15.619	30.54
3.730	32.22	0.1158	56.020	22.4	794.4	9059.0498	10000	0.1950	0.7655	11324	1.1324E6	3.384E-3	0.9	3.5	207.020	11.445	25.77
2.671	25.83	0.1034	57.008	22.4	806.0	9082.7197	10000	0.1978	1.208	11353	1.1353E6	3.384E-3	1.0	3.5	208.008	8.1943	20.67
2.006	22.04	0.09100	58.004	22.4	796.9	9094.2998	10000	0.1956	1.641	11368	1.1368E6	3.384E-3	1.0	3.5	209.004	6.1532	17.63
0.8835	13.51	0.06540	59.016	22.4	783.7	9110.9502	10000	0.1923	4.294	11389	1.1389E6	3.384E-3	1.0	3.5	210.016	2.7104	10.81
0.1718	6.134	0.02801	60.004	22.4	780.4	9118.7402	10000	0.1915	20.74	11398	1.1398E6	3.383E-3	1.0	3.5	211.004	0.52704	4.907

